Ionizing Radiation Division

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Instrument Development for X-Ray Spectroscopy

We design and fabricate novel x-ray instrumentation for specific internal and external applications. Internal to the Physics Laboratory, we have deployed high resolution crystal diffraction instruments at the NIST EBIT. We developed a spectroscopic package for non-invasive high voltage measurement with particular reference to mammographic quality control. In space-based applications we provided crystals for several missions including P78-1, Solar Max, and Astro D (Yohkoh). In addition we built and delivered double crystal monochromators to NASA GSFC for calibration of XTE and to support cryogenic x-ray detector development. One version of this pentagonal turret design was used at MSFC for final test and calibration of the Chandra X-Ray Telescope We are currently working on instrument designs for diagnostic studies of plasma sources at the Rochester LLE and the Livermore NIF.

Quantum Metrology:
Instrument Development for X-Ray Spectroscopy
Thin Film and Multilayer Metrology
X-Ray and Gammay-Ray Metrology

Curved Crystal Transmission Spectometer

schematic of crystal spectrometer
Schematic of crystal spectrometer

This effort specializes in designing, fabricating, and testing innovative crystal spectrometers for a variety of scientific and technological applications. One recent design that has found a variety of uses is shown schematically above. X-rays from a source are dispersed and focussed by a curved crystal used in transmission through a central, background-suppressing aperture onto a fixed image plane. Two mirror-symmetric spectra are imaged, in this case on a size 2 CCD dental sensor, and a spectrum is constituted by pixel column summing as shown to the right. The distance between identical features can be converted to energy via a predetermined plate function of the form E=1/sqrt(a/(x*x) +b) where a and b are constants and x is the distance from the center of the detector. Relative to a flat crystal instrument, the curved-crystal design provides insensitivity to source size, enhanced spectral dispersion and, because of the focusing action of the bent crystal, increased efficiency.

We recently patented this design for the noninvasive determination of the applied high voltage of mammographic x-ray sources which is accomplished by measuring the high-energy cutoff of the continuum spectrum. Since the entire spectral distribution is registered, the effects of added filtration and target and window contamination can also be studied. Designs have also been adopted as core plasma diagnostics for high-power laser studies at the Laboratory for Laser Energetics (LLE) in Rochester, NY and at the National Ignition Facility (NIF) at Lawrence Livermore National Laboratory in collaboration with NRL. For more detailed information see the NRL spectroscopy web site. The design has also been applied by other researchers toward the measurement of the 1s Lamb shift in hydrogenic uranium at GSI in Darmstadt, Germany. Additional applications are being pursued, including characterization of pulsed laser sources used in medical applications.

view larger image Top: False color image from a quartz-crystal spectrometer acquired with a size-2 dental CCD with 524 × 760 pixels. A pinhole-camera image of the focal spot is visible in the center of the image.

Bottom: The pixel column sum plot or spectrum of the image shown above. This shows the molybdenum spectrum (the alpha lines are saturated), broad-band continuum radiation, and the image of the focal spot in the center (shown with an expanded vertical scale). The high-energy cutoff of the spectrum is marked by arrows and, through the dispersion function, gives the high-voltage applied to the x-ray tube. (Larger view)

Curved Crystal Reflection Instrument for EBIT Spectroscopy

We are pursuing a research program of crystal spectrometry at the NIST EBIT. Here development emphasis is being directed toward novel optical arrangements and detection schemes. The electron beam ion trap (EBIT) is a small-scale laboratory instrument that uses a tightly focused and energy-tunable electron beam to create, trap, and probe highly charged ions.

EBIT spectra Spectra acquired at the NIST EBIT of Ne-like Xe and, using a metal vapor vacuum arc (MEVVA), He-like Ti.

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Online: September 2000   -   Last update: December 2005